What is the role of ammonium bifluoride (ABF) in the extraction of tantalum (Ta) and niobium (Nb) from coltan-bearing ore?
Label:chem
Topic
Ammonium bifluoride (ABF, NH4F·HF) is a strong fluorination agent used in the extraction of transition and refractory metals like tantalum (Ta) and niobium (Nb). It is known for its reactivity similar to that of fluorine and hydrofluoric acid (HF), but it is safer to transport and handle. ABF is non-volatile at room temperature and environmentally safe. It is relatively inexpensive and can be recycled from gaseous compounds.
Answer
Ammonium bifluoride (ABF) is used as a fluorination agent to pre-treat coltan-bearing ore, converting the Ta and Nb oxides into water-soluble ammonium fluorides. This process enhances the subsequent sulfuric acid leaching efficiency, allowing for high recovery rates of Ta and Nb. The optimal conditions for this process include an ABF-ore mass ratio of 5/1, a fluorination temperature of 200°C, and a fluorination duration of 2.5 hours, resulting in about 94% recovery of Ta and 95% recovery of Nb.
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